EF-G in Complex with GDP and the Ribosome in Thermus thermophilus

Zac LaRocca-Stravalle '21 and Kylie Writer '21


Contents:


I. Introduction

Model View:


Elongation Factor G (EF-G) is a prokaryotic translation factor involved in the catalysis of translocation. As part of the guanosinetriphosphatase (GTPase) superfamily, EF-G functions via guanosine triphosphate (GTP) binding. In this complex, EF-G�GTP binds to the ribosome and catalyzes the translocation of peptidyl-tRNA from the aminoacyl (A) site to the peptidyl (P) site in the small subunit (30S) of the ribosome. As this occurs, a single mRNA codon shifts 5� to 3� relative to the ribosome. After translocation is complete, GTP is hydrolyzed to guanosine diphosphate (GDP) and a conformational change occurs in the EF-G complex. In this new conformation, the EF-G�GDP complex dissociates from the ribosome and subsequently forms a complex with GTP in a catalytic cycle (Al-Karadaghi et al., 1996).

The EF-G�GDP complex has important structural interactions in the translocation process. The conformational change induced by GTP hydrolysis is extensive in EF-G�GDP, and its interaction with the ribosome also contribute to such changes. In this tutorial, we will identify the basic components of EF-G as well as the major interaction sites and structural changes with regard to GDP and the ribosome.  


II. General Structure

The three dimensional structure of EF-G is presented to the left. In this structure, EF-G is in the GDP complex conformation. EF-G is made up of 691 amino acid residues with a molecular weight of ~80 kDa and a length of ~110 �; it is the largest GTPase known (Jurnak et al., 1994). The of EF-G is made up of 19 alpha helices (177 residues; 25%) and 42 beta sheets (217 residues; 31%). EF-G can be broken into 5 : G domain (N-terminal), domain II, domain III, domain IV (C-terminal), and domain V . The : can be further divided into the G core subdomain and the G insert subdomain (G�); both GTP and GDP bind at the G core (Czworkowskil, et al.,1994; Al-Karadaghi, et al., 1996). All domains make contact with the ribosome. Both domain II and domain III contact with the 30S subunit of the ribosome, with further contact in the 50S subunit by domain III. Domain V primarily contacts the 50S subunit. Domain IV, inserted into the 30S subunit, interacts with the P-site tRNA and mRNA. 


III. GDP Binding

binds to the G core subdomain at the nucleotide-binding site. The two phosphates of GDP interact with the main chain atoms in the (residues 19-26), while the ribose sugar and guanine base interact with the side chain residues in the G core domain (Al-Karadaghi et al., 1996). The specific residues that interact with GDP, via hydrogen bonding, are as follows:

:

Beta Phosphate:

Asp 22 (N) interacts with O23.

Gly24 (N) and Ala 23 (N) interact with O21.

Thr26 (N) and Lys 25 (N) interact with O22.

Alpha Phosphate:

Thr 27 (OG1 and N) interact with O13.

:

Lys 138 (N) interacts with O4'.

:

Asn 137 (N) interacts with N7.

Ser 262 (O) and Ala 263 (N) interact with O6.

Asp 140 (OD1 and OD2) interact with N1 and N2 respectively.
 


IV. GDP Induced Conformational Changes

Studies comparing EF-G�GDP with EF-G in the nucleotide free state have noted the local changes around the nucleotide-binding site. Upon incorporation of GDP, a conformational flip occurs in the P-loop, leading to the displacement of (residues 116�123) and the (residues 85�100) as well as in parts of domains III, VI, and V. The specific amino acid changes are described as follows: when GDP enters the site, it forces the displacement of in the P-loop. The of IIe21 that would normally occupy the position of the beta phosphate of GDP gets moved 5.4 �, 3.1 � from N delta 1 of His20, in GDP occupancy. The between the O delta 2 of Asp22 and N delta 1 of His20 is then replaced by to N zeta of Lys138. Additionally, Ile21 and Asp22 get rotated 180�.


Despite this change, the P-loop maintains stabilization after GDP incorporation. This can be attributed, in part, to the unchanged hydrogen bond distance of His20 and . His20 and Gln117 move positions with respect to other residues, and this induces a displacement in the helix CG from its position in the nucleotide free state. The CG is then packed between helix BG and the domain V. Both the changes in the P-loop and helix CG affect switch II region. The switch II region is important for the conformational changes during GTP hydrolysis to GDP in GTPases, and this has been shown in EF-Tu (Kjeldgaard et al., 1993). When comparing EF-G�GDP with the nucleotide free state, however, the switch II region does not cause as much conformational transitions as it might after GTP hydrolysis (Al-Karadaghi et al., 1996). Nonetheless, EF-G binding of the ribosome is associated with its own interactions, and they may contribute to the conformational changes seen in EF-G between the pre-translocation and post-translocation ribosome (Gao et al., 2009).  


V. Ribosome Binding


EF-G is known to have different conformational states in the ribosome. As described, the structure of EF-G is influenced by whether it is bound to a phosphorylated nucleotide, and if so, whether it is bound to GTP or GDP. However, the interaction with the ribosome also contributes to conformational changes in EF-G in tandem with GTP hydrolysis. There are two major structural changes seen in the EF-G ribosome complex: the compact and elongated forms. The compat form is associated with GTP binding and pre-translocation; the elongated form is associated with GDP and post-translocation, similar to what is shown in the three-dimensional structure to the left. Nevertheless, it remains unclear how exactly GTP hydrolysis in EF-G is coupled with the pre- and post-translational ribosome (Lin et al., 2015).

The binding of EF-G to the ribosome is similar to other GTPases, namely, EF-Tu in complex with GTP. The major binding sites of EF-G and the ribosome are specific. The G domain, domain III, and domain V surround the sarcin-ricin loop of the ribosome. Domain III makes with the 30S subunit, and domain V contacts the 50S subunit. Along with Domain III, also contacts the 30S subunit and experiences numerous interactions and structural changes. From the compact to the elongated form, domain IV experiences a 90 degree rotation into the A-site of the ribosome that mimics the tRNA moiety, and makes substantial contacts with the ribosome, tRNA and mRNA. Domain IV contains that facilitate binding interaction: loop I (residues 496 to 509) and loop II (residues 567 to 579). Before the IV domain occupies the A site, two (residues 502 and 503) help flip loop I into the P-site between the tRNA and codon. Among other interactions, domain IV plays a major role the EF-G ribosome complex.


VI. References

Salam Al-Karadaghi, Arnthor �varsson, Anders Liljas, Maria Garber, and Julia Zheltonosova. 1996. The structure of elongation factor G in complex with GDP: conformational flexibility and nucleotide exchange. Structure Volume 4, Issue 5 495-637.

J.Czworkowskil, J.Wang, T.A.Steitz1, and P.B.Moore1. 1994. The crystal structure of elongation factor G complexed with GDP, at 2.7 A resolution The EMBO Journal vol.13 no.16 pp.3661-3668.

Yong-Gui Gao, Maria Selmer, Christine M. Dunham, Albert Weixlbaumer, Ann C. Kelley, and V. Ramakrishnan. 2009. The Structure of the Ribosome with Elongation Factor G Trapped in the Posttranslocational State. Science Vol. 326, Issue 5953, pp. 694-699.

Rajendra K. Agrawal, Pawel Penczek, Robert A. Grassucci, and Joachim Frank. 1998. Visualization of elongation factor G on the Escherichia coli 70S ribosome: The mechanism of translocation PNAS 95(11)6134-6138.

A.Avarsson, E.Brazhnikov1, M.Garberl, J.Zheltonosova Yu.Chirgadze, S.AI-Karadaghi, L.A.Svensson, and A.Liljas. 1994. Three-dimensional structure of the ribosomal translocase: elongation factor G from Thermus thermophilus The EMBO Journal vol.13 no.16 pp.3669-3677.

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